Water → HCID 178457123, 화합물

HRID 1577535

반응식

HRID 1577535 반응식
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.P(Cl)(Cl)(Cl)(Cl)Cl.[CH2:25]([NH2:28])[CH:26]=[CH2:27].O>C(OCC)(=O)C>[CH2:25]([NH:28]/[C:1](/[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)=[C:9]1\[C:10](=[O:18])[C:11]2[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=2[S:13]\1)[CH:26]=[CH2:27]

참가 물질

6

반응물 4

HCID 962WaterHCID 7853AllylamineHCID 24819Phosphorus pentachlorideHCID 4712192Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl-

생성물 1

HCID 178457123HCID 178457123, 화합물수율 43%

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

Prepared as in Example 1 from 2-benzoyl-benzo[b]thiophen-3-ol, phosphorus(V) chloride and a solution of one part by volume of allylamine in 2 parts by volume of water with a yield of 43% of theory. M.p. 104°-106° C. (ethyl acetate).

출처 및 근거

ORD 기록
ord-1b0dab7777a145188dd7f872712b4f3f
출처 데이터셋
uspto-grants-1981_09
특허 번호
US04288437

연결된 노트

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