Hexamethylenediamine → N-phenylstearyl hexamethylene diamine

HRID 1578428노트

반응식

HRID 1578428 반응식
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24]Br)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH2:33]>C(O)C>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][NH:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH2:33])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

4

반응물 2

HCID 16402HexamethylenediamineHCID 53680545HCID 53680545, 화합물

생성물 1

HCID 86733042N-phenylstearyl hexamethylene diamine

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Following the procedure of Example XVI a solution of 15.8 grams (0.04 mole) of phenylstearyl bromide and 37.2 grams (0.32 mole) of hexamethylene diamine in 400 ml of ethanol was refluxed for three hours. After the same recovery procedure 15.2 grams (88.4% crude mass yield) of N-phenylstearyl hexamethylene diamine was obtained having the following analysis:

후처리

  1. temperaturewas refluxed for three hours

출처 및 근거

ORD 기록
ord-a40055875796432c81ab38d600664d83
출처 데이터셋
uspto-grants-1976_02
특허 번호
US03936503

반응 노트

불러오는 중…