4,6-Dichloro-1,3,5-trazin-2-amine → HCID 21558473, 화합물

반응식

[Cl:1][CH:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4](C)[N:3]1N.ClC1N=C(Cl)N=C(N)N=1.ClC1N=C(Cl)N=[C:23]([NH:28][C:29]([NH2:31])=[O:30])N=1>>[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([N:28]([CH3:23])[C:29]([NH2:31])=[O:30])[N:3]=1

참가 물질

반응물 3

HCID 136154,6-Dichloro-1,3,5-trazin-2-amine

HCID 11298723Urea, (4,6-dichloro-1,3,5-triazin-2-yl)-

HCID 70306188HCID 70306188, 화합물

생성물 1

HCID 21558473HCID 21558473, 화합물

실험 절차

By using 89 parts of 2,4-dichloro-6-methyl-amino-s-triazine instead of 82.5 parts of 2,4-dichloro-6-amino-s-triazine and otherwise carrying out the procedure as described in Example 1 for the manufacture of N-(2,4-dichloro-s-triazin-6-yl)-urea, there are obtained 79.5 parts of N-(2,4-dichloro-s-triazin-6-yl)-N-methyl-urea with a melting point of 172°-174°C.

출처 및 근거

ORD 기록: ord-699c7894ef624825a3644e4b3ad3fbc2
출처 데이터셋: uspto-grants-1976_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03939158

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