Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxygen → Trioctyl phosphate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxygen | HCID 977 | — |
| 반응물 | Octyl phosphite | HCID 76413 | — |
| 촉매 | Cobalt octoate | HCID 8696 | — |
| 생성물 | Trioctyl phosphate | HCID 15733 | 91% |
반응 단계
A mixture of 0.2 g. of cobalt octoate and 70 g. of trioctyl phosphite is warmed in vacuo (10 mm.) at 30°C while oxygen is added over a period of six hours. The mixture is stirred throughout this period by means of a magnetic stirrer. The product is washed with an aqueous alkaline solution to remove the cobalt catalyst, having a 91% yield of trioctyl phosphate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03939229 |
| 출처 데이터셋 | uspto-grants-1976_02 |
| ORD ID | ord-872a2dab69c84d7d96c8950da038a833 |
| 출처 메모 | uspto-grants-1976_02 |