HCID 131710058, 화합물 → HCID 21557324, 화합물

HRID 1578928노트

반응식

HRID 1578928 반응식
Cl.[CH3:2][C:3]([C:5]1[C:10]([C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][CH:12]=2)=[C:9]([NH2:18])[N:8]=[C:7]([NH2:19])[N:6]=1)=[O:4]>O>[CH3:2][C:3]([C:5]1[C:10]([C:11]2[CH:12]=[CH:13][C:14]([Cl:17])=[CH:15][CH:16]=2)=[C:9]([NH2:18])[N:8]=[C:7]([NH2:19])[N:6]=1)=[O:4]

참가 물질

3

반응물 1

HCID 131710058HCID 131710058, 화합물

생성물 1

HCID 21557324HCID 21557324, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A sample of [2,6-diamino-5-(p-chlorophenyl)-4-pyrimidinyl] methyl ketone, hydrochloride was dissolved in water and then precipitated with concentrated NH4OH to give the title compound, m.p. 206°-208°.

후처리

  1. customprecipitated with concentrated NH4OH

출처 및 근거

ORD 기록
ord-dd58c6670d4f42e1bdc86e01ee2a3cab
출처 데이터셋
uspto-grants-1976_02
특허 번호
US03940393

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