Acetohydrazide → HCID 178475140, 화합물
반응식
[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10](=[NH:14])OCC.[C:15]([NH:18][NH2:19])(=[O:17])[CH3:16]>CO>[CH3:1][N:2]1[C:6]([N+:7]([O-:9])=[O:8])=[CH:5][N:4]=[C:3]1[C:10]([NH:19][NH:18][C:15](=[O:17])[CH3:16])=[NH:14]참가 물질
4
실험 절차
In 200 ml. of methanol, 12 g. (0.06 mole) of ethyl 1-methyl-5-nitro-2-imidazolecarboximidate and 4.9 g. (0.066 mole) of acetyl hydrazine are refluxed for 30 hours. The yellow compound is collected, washed with cold methanol and dried to give 12.97 g. of the title compound, melting point 294°C.
후처리
- customThe yellow compound is collected
- washwashed with cold methanol
- customdried
- customto give 12.97 g
출처 및 근거
- ORD 기록
- ord-6646db82708743fe97c41ba1da41885f
- 출처 데이터셋
- uspto-grants-1976_02
- 특허 번호
- US03940411
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