Cyclooctanone → HCID 21567553, 화합물

HRID 1579167노트

반응식

[C:1]([NH:5][NH:6][C:7]([C:12]#[N:13])([CH:9]1[CH2:11][CH2:10]1)[CH3:8])([CH3:4])([CH3:3])[CH3:2].[C:14]1(=O)[CH2:21]CCCCC[CH2:15]1.C1(C(C)=O)CC1>>[C:1]([NH:5][NH:6][C:7]1([C:12]#[N:13])[CH2:8][CH2:21][CH2:14][CH2:15][CH2:10][CH2:11][CH2:9]1)([CH3:2])([CH3:3])[CH3:4]

참가 물질

반응물 3

HCID 10403Cyclooctanone

HCID 13004Cyclopropyl methyl ketone

HCID 23344788HCID 23344788, 화합물

생성물 1

HCID 21567553HCID 21567553, 화합물수율 100%

실험 절차

1-t-Butylhydrazo-1-cyanocyclooctane was prepared in 100% yield using the same procedure described in Example XIIIB for the preparation of 1-t-butylhydrazo-1-cyano-1-cyclopropylethane, substituting the t-butylhydrazone of cyclooctanone for the t-butylhydrazone of methyl cyclopropyl ketone.

출처 및 근거

ORD 기록: ord-154d895bc30f47259ae35700411c8bcc
출처 데이터셋: uspto-grants-1976_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03931143

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