Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminobenzoic Acid → 4-(1-Cyclohexene-1-carbonylamino)-benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminobenzoic Acid | HCID 978 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1-Cyclohexenecarbonyl chloride | HCID 142066 | — |
| 생성물 | 4-(1-Cyclohexene-1-carbonylamino)-benzoic acid | HCID 21486323 | — |
반응 단계
88.0%. B. 4-(1-cyclohexene-1-carbonylamino)-benzoic acid was prepared as described in Example 1 from 16.6 g (0.121 mol) of p-aminobenzoic acid with 22.0 g (0.152 mol) of 1-cyclohexene-1-carboxylic acid chloride and 21.3 ml (0.152 mol) of triethylamine. Recrystallization from THF/n-pentane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03931153 |
| 출처 데이터셋 | uspto-grants-1976_01 |
| ORD ID | ord-1b4f930b1f344eb1bb37ea873bd3d194 |
| 출처 메모 | uspto-grants-1976_01 |