N-(3-Chloropropyl)dibutylamine → Bis(3-dibutylaminopropyl) 9-ethylcarbazole-3,6-dicarboxylate dihydrochloride

HRID 1580165

반응식

HRID 1580165 반응식
[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([OH:18])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([OH:21])=[O:20])[CH:8]=2)[CH3:2].[CH2:22]([N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:27][CH2:28][CH2:29][Cl:30])[CH2:23][CH2:24][CH3:25]>[Cl-].C([N+](C)(C)C)C1C=CC=CC=1>[ClH:30].[ClH:30].[CH2:1]([N:3]1[C:15]2[CH:14]=[CH:13][C:12]([C:16]([O:18][CH2:29][CH2:28][CH2:27][N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:22][CH2:23][CH2:24][CH3:25])=[O:17])=[CH:11][C:10]=2[C:9]2[C:4]1=[CH:5][CH:6]=[C:7]([C:19]([O:21][CH2:29][CH2:28][CH2:27][N:26]([CH2:31][CH2:32][CH2:33][CH3:34])[CH2:22][CH2:23][CH2:24][CH3:25])=[O:20])[CH:8]=2)[CH3:2]

참가 물질

4

반응물 2

HCID 96084N-(3-Chloropropyl)dibutylamineHCID 37979149-ethyl-9H-carbazole-3,6-dicarboxylic acid

생성물 1

HCID 68134129Bis(3-dibutylaminopropyl) 9-ethylcarbazole-3,6-dicarboxylate dihydrochloride

시약·촉매·용매 1

HCID 5963Benzyltrimethylammonium chloride촉매

실험 절차

By the procedure of Example 2, one equivalent of 9-ethylcarbazole-3,6-dicarboxylic acid is allowed to react with two equivalents of 3-dibutylaminopropylchloride in the presence of a catalytic amount of benzyltrimethylammonium chloride to give the product.

후처리

  1. customto give the product

출처 및 근거

ORD 기록
ord-afdfcb0c8be04e5c995ea9bef13f1e56
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03932456

연결된 노트

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