참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | 1-Iodo-3-triphenylmethoxy-trans-1-octene | HCID 20144636 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | HCID 178506898 | HCID 178506898 | — |
반응 단계
To a solution of 4.96 g. of 1-iodo-3-triphenylmethoxy-trans-1-octene (Example 730) in 10 ml. of toluene cooled to -78°C. is added under an inert atmosphere 1 molar equivalent of n-butyllithium dissolved in hexane. The reaction mixture is allowed to warm to -40°C. and is then maintained at that temperature for 1hour to yield a hydrocarbon solution of 3-triphenylmethoxy-trans-1-octenyllithium.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03932479 |
|---|
| 출처 데이터셋 | uspto-grants-1976_01 |
|---|
| ORD ID | ord-8707e8110a13498db0df5a106c014b3e |
|---|
| 출처 메모 | uspto-grants-1976_01 |
|---|
