Benzyl Bromide → HCID 12255191, 화합물

HRID 1580635노트

반응식

HRID 1580635 반응식
[Br:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[NH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1>C1(C)C(C)=CC=CC=1>[Br-:1].[NH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N+:11]=1[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

4

반응물 2

HCID 7498Benzyl BromideHCID 104392-Aminopyridine

생성물 1

HCID 12255191HCID 12255191, 화합물수율 63.9%

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

A solution of α-bromotoluene (100.0 g), 2-aminopyridine (82.0 g) and 1000 ml of xylene are heated under reflux for 7 hours to give 99.1 g of the title compound, melting point 187°-190°C.

후처리

  1. temperatureunder reflux for 7 hours

출처 및 근거

ORD 기록
ord-8f37d51154d7488085a0ccefe10ad9a6
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03933836

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