Sodium Methoxide → HCID 4961624, 화합물

HRID 1580636노트

반응식

HRID 1580636 반응식
[Br-].[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][N+:4]=1[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.C[O-].[Na+]>CO>[C:10]1([CH2:9][N:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]2=[NH:2])[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

참가 물질

4

반응물 2

HCID 10942334Sodium MethoxideHCID 12255191HCID 12255191, 화합물

생성물 1

HCID 4961624HCID 4961624, 화합물수율 96.6%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a solution of 2-amino-1-(phenylmethyl)pyridinium bromide (94.5 g) in 700 ml of methanol is added, portionwise, a total of 38.5 g of sodium methoxide. The mixture is stirred and heated under reflux conditions for 2.5 hours. Workup yields 63.4 g of the title compound, melting point 52°-54°C.

후처리

  1. temperatureheated under reflux conditions for 2.5 hours

출처 및 근거

ORD 기록
ord-05cddba18ef04aaa81610aead1167f91
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03933836

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