Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 4-Amino-2-chlorobenzenesulfonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-Chloro-3-nitrobenzene | HCID 8489 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Sodium Sulfite | HCID 24437 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-Amino-2-chlorobenzenesulfonic acid | HCID 15850359 | — |
반응 단계
A mixture of 31.5 grams of 3-chloronitrobenzene, 450 milliliters of 5N-sodium sulphite solution and 500 milliliters of 2N sodium hydroxide solution was refluxed with stirring for 90 minutes, acidified with concentrated hydrochloric acid, and refluxed for 1 hour. On cooling and diluting with water a solid crystallised out which was filtered and washed with water to give 9.9 grams of 2-chlorosulphanilic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03933829 |
| 출처 데이터셋 | uspto-grants-1976_01 |
| ORD ID | ord-3ea4c2676db44e6caef9821dde52820b |
| 출처 메모 | uspto-grants-1976_01 |