3',4',5'-Trimethoxyacetophenone → HCID 56638083, 화합물

HRID 1580940

반응식

HRID 1580940 반응식
C[O-].[Na+].[CH3:4][C:5]1[N:6]=[C:7]2[C:16]([CH3:17])=[CH:15][CH:14]=[CH:13][N:8]2[C:9](=[O:12])[C:10]=1[CH3:11].[CH3:18][C:19]([C:21]1[CH:26]=[C:25]([O:27][CH3:28])[C:24]([O:29][CH3:30])=[C:23]([O:31][CH3:32])[CH:22]=1)=O>CO>[CH3:11][C:10]1[C:9](=[O:12])[N:8]2[CH:13]=[CH:14][CH:15]=[C:16]([CH3:17])[C:7]2=[N:6][C:5]=1[CH:4]=[C:19]([CH3:18])[C:21]1[CH:22]=[C:23]([O:31][CH3:32])[C:24]([O:29][CH3:30])=[C:25]([O:27][CH3:28])[CH:26]=1

참가 물질

5

반응물 3

HCID 143453',4',5'-TrimethoxyacetophenoneHCID 10942334Sodium MethoxideHCID 123397192,3,9-Trimethyl-4H-pyrido[1,2-a]pyrimidin-4-one

생성물 1

HCID 56638083HCID 56638083, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a solution of 1.3g of sodium methoxide in 75 ml of absolute methanol is added 2.0g of 2,3,9-trimethyl-4H-pyrido[1,2-a]pyrimidin-4-one, followed by 4.2g of 3,4,5-trimethoxyacetophenone. The mixture is stirred and heated under reflux for 97 hours to yield the title compound.

후처리

  1. temperatureheated
  2. temperatureunder reflux for 97 hours

출처 및 근거

ORD 기록
ord-3b46f4bd6cd34af7aedd772a6e636d2e
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03935197

연결된 노트

불러오는 중…