Fumaric Acid → HCID 20260340, 화합물

HRID 1583289노트

반응식

HRID 1583289 반응식
[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([C:12]3[CH:13]([CH3:19])[CH2:14][C:15](=[O:18])[NH:16][N:17]=3)=[CH:8][CH:7]=2)[CH:5]=[CH:4][N:3]=[CH:2]1.[C:20]([OH:27])(=[O:26])/[CH:21]=[CH:22]/[C:23]([OH:25])=[O:24]>C(O)C>[C:20]([OH:27])(=[O:26])/[CH:21]=[CH:22]/[C:23]([OH:25])=[O:24].[N:1]1([C:6]2[CH:7]=[CH:8][C:9]([C:12]3[CH:13]([CH3:19])[CH2:14][C:15](=[O:18])[NH:16][N:17]=3)=[CH:10][CH:11]=2)[CH:5]=[CH:4][N:3]=[CH:2]1

참가 물질

4

반응물 2

HCID 444972Fumaric AcidHCID 30217294,5-dihydro-6-(4-(imidazol-1-yl)phenyl)-5-methyl-3(2H)-pyridazinone

생성물 1

HCID 20260340HCID 20260340, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of 5 g of 6-[4-(1-imidazolyl)-phenyl]-5-methyl-3-oxo-2,3,4,5-tetrahydropyridazine and 2.3 g of fumaric acid was heated in 250 ml of ethanol until the solid had all dissolved. The solution was then evaporated to dryness, and the residue was dried.

후처리

  1. customThe solution was then evaporated to dryness
  2. customthe residue was dried

출처 및 근거

ORD 기록
ord-94627c12b6c24bef9677c7780948f554
출처 데이터셋
uspto-grants-1985_11
특허 번호
US04551455

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