Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1583724생성일: 2026년 10월 27일
N-((Phenylmethoxy)carbonyl)-L-alanyl-L-alanine → Benzyloxycarbonylalanyl-alanyl Proline Ethylamide
https://huagongshe.com/reaction/1583724
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N-((Phenylmethoxy)carbonyl)-L-alanyl-L-alanine | HCID 7009583 | — |
| 반응물 | Proline ethylamine | HCID 70479868 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Benzyloxycarbonylalanyl-alanyl Proline Ethylamide | HCID 13750000 | — |
반응 단계
11 grams of N,N-dicyclohexylcarbodiimide was added to a solution of 14.7 grams of benzyloxycarbonylalanyl alanine in 100 ml of dimethylformamide and 7.6 g of proline ethylamine (prepared from the corresponding benzyloxycarbonyl derivative) cooled to -5 degrees C. and the reaction mixture treated by conventional techniques. 10.6 g of product having a melting point of 139 to 140 degrees C. was obtained. [α]D20 -46.5 degrees (c 0.3; dimethylformamide).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04554100 |
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| 출처 데이터셋 | uspto-grants-1985_11 |
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| ORD ID | ord-d31229fcf48e40f89b133e52964b1a19 |
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| 출처 메모 | uspto-grants-1985_11 |
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