Phosgene → HCID 13535829, 화합물

HRID 1583753노트

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HRID 1583753 반응식
[CH3:1][CH:2]1[CH2:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([NH:11][NH:12][C:13]([N:15]([O:17][CH3:18])[CH3:16])=[O:14])[C:4]=2[O:3]1.[C:19](Cl)([Cl:21])=[O:20]>C1C=CC=CC=1>[Cl:21][C:19]([N:11]([C:10]1[C:4]2[O:3][CH:2]([CH3:1])[CH2:6][C:5]=2[CH:7]=[CH:8][CH:9]=1)[NH:12][C:13]([N:15]([O:17][CH3:18])[CH3:16])=[O:14])=[O:20]

참가 물질

4

반응물 2

HCID 6371PhosgeneHCID 135358281-(2,3-Dihydro-2-methylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazide

생성물 1

HCID 13535829HCID 13535829, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

3.0 g of 1E was added to a stirred solution of 75 ml of 12.5% phosgene in benzene. The resulting mixture was stirred for 2 hours at room temperature, then the solvent was evaporated to give 1-(chlorocarbonyl)-1-(2,3-dihydro-2-methylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazide (1F), as an amber syrup.

후처리

  1. customthe solvent was evaporated

출처 및 근거

ORD 기록
ord-4d8dff9d476a411a80d54c86637d488e
출처 데이터셋
uspto-grants-1985_11
특허 번호
US04554283

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