Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethylbutyraldehyde | HCID 7359 | — |
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 생성물 | 3,7-Diethyl-5-azanona-3,5-diene | HCID 12413470 | 76.5% |
반응 단계
To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene. Mass spectrum m/e=181. 13C nuclear magnetic resonance spectrum, solvent CDCl3, ref. TMS. ##STR7##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04555576 |
| 출처 데이터셋 | uspto-grants-1985_11 |
| ORD ID | ord-546100d3352a4001a06fac0ff0155d98 |
| 출처 메모 | uspto-grants-1985_11 |