Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylimidazole → 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylimidazole | HCID 12749 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 6-Chloropiperonyl chloride | HCID 90113 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-((6-chloro-1,3-benzodioxol-5-yl)methyl)2-methyl-1H-imidazole | HCID 21224807 | — |
반응 단계
The operation is carried out as in Stage 1 of Example 11 starting with 12.3 g of 2-methyl-1H-imidazole, 7.92 g of sodium hydride with 50% oil, 150 ml of N dimethylformamide and 33.8 g of 6-chloropiperonyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05932741 |
| 출처 데이터셋 | uspto-grants-1999_08 |
| ORD ID | ord-6b398965cfb84cc889a194adca6f3e3c |
| 출처 메모 | uspto-grants-1999_08 |