(4-chloro-2-Methylphenoxy)acetic acid → (4-chloro-2-Methylphenoxy)acetic acid

HRID 1585830노트

반응식

HRID 1585830 반응식
[OH-].[K+:2].[CH3:3][C:4]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:5]=1[O:11][CH2:12][C:13]([OH:15])=[O:14]>>[CH3:3][C:4]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:5]=1[O:11][CH2:12][C:13]([O-:15])=[O:14].[K+:2].[CH3:3][C:4]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:5]=1[O:11][CH2:12][C:13]([OH:15])=[O:14]

참가 물질

4

반응물 2

HCID 7204(4-chloro-2-Methylphenoxy)acetic acidHCID 14797Potassium Hydroxide

생성물 2

HCID 7204(4-chloro-2-Methylphenoxy)acetic acidHCID 23682017Potassium (4-chloro-2-methylphenoxy)acetate

실험 절차

6.6 parts (0.1 mol) of powdered potassium hydroxide (85%) are introduced into a melt of 20 parts (0.1 mol) of MCPA (93.3%) with stirring and the mixture is kept at 130° C. for 30 minutes. After solidification, 26 parts of MCPA-potassium having an MCPA content of 71.8% are obtained, which corresponds to a yield of 100%. M.p.: 203° C.

출처 및 근거

ORD 기록
ord-da9afdd0d8a24be3b24a8caa4d5f8bec
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05939584

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