Diethyl Ether → HCID 178488142, 화합물

HRID 1586472노트

반응식

[CH3:1][O:2][C:3]1[CH:20]=[CH:19][C:6]2[NH:7][C:8]([S:10][CH2:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH2:18])=[N:9][C:5]=2[CH:4]=1.C([O:23]CC)C>>[CH3:1][O:2][C:3]1[CH:20]=[CH:19][C:6]2[NH:7][C:8]([S:10]([CH2:11][C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=3[NH2:18])=[O:23])=[N:9][C:5]=2[CH:4]=1

참가 물질

반응물 2

HCID 3283Diethyl Ether

HCID 178488113HCID 178488113, 화합물

생성물 1

HCID 178488142HCID 178488142, 화합물

실험 절차

The title compound was prepared by the method of Example 3 using 1.20 g of the title product of Example 11 instead of the title product of Example 2. Trituration with diethylether gave 1.04 g of the title compound: m.p. 147-148° C. Anal. Calc'd. for C15H15N3O2S: C, 59.78; H, 5.02; N,13.94; S, 10.64. Found: C, 59.30; H, 4.95; N, 13.55; S, 10.73.

출처 및 근거

ORD 기록: ord-056f4435fe79446abc657c5b70f7524a
출처 데이터셋: uspto-grants-1999_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05945425

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