Diethyl Ether → HCID 69796367, 화합물

HRID 1586478노트

반응식

[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20].C([O:23]CC)C>>[OH2:23].[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20])=[O:23].[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[C:14]([CH3:19])[C:13]=1[NH2:20])=[O:23]

참가 물질

반응물 2

HCID 3283Diethyl Ether

HCID 14064669HCID 14064669, 화합물

생성물 1

HCID 69796367HCID 69796367, 화합물

실험 절차

The title compound was prepared by the method of Example 3 using 950 mg of the title product of Example 29 instead of the title product of Example 2. Trituration with diethylether gave 434 mg of the title compound. Anal. Calc'd. for C16H17N3OS*1/2H2O: C, 62.23; H, 5.88; N, 13.63; S, 10.40. Found: C, 62.39; H, 5.72; N, 13.50; S, 10.65.

출처 및 근거

ORD 기록: ord-70db90bd557e427c849a1f09bec9d94a
출처 데이터셋: uspto-grants-1999_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05945425

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