Methanesulfonyl chloride → 2-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

HRID 15873노트

반응식

HRID 15873 반응식
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[CH2:5][CH2:6][OH:7].[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:7][CH2:6][CH2:5][C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([NH:1][S:12]([CH3:11])(=[O:14])=[O:13])[CH:3]=1)(=[O:14])=[O:13]

참가 물질

3

반응물 2

HCID 31297Methanesulfonyl chlorideHCID 149389872-(3-Aminophenyl)ethan-1-ol

생성물 1

HCID 574443592-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

실험 절차

The title compound was prepared from 3-aminophenethyl alcohol (U.S. Pat. No. 2,641,602) and methanesulfonyl chloride (2 eq.) according to the procedure contained within description 4. The product was used immediately without further purification or characterisation.

후처리

  1. customThe product was used immediately without further purification or characterisation

출처 및 근거

ORD 기록
ord-df39bbbc55b94cc4a4671516af5755d6
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07732600B2

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