Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Pyrrolidone → 1-[3-(2-Hydroxyethyl)phenyl]-2-pyrrolidinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Pyrrolidone | HCID 12025 | — |
| 반응물 | 2-(3-Bromophenyl)ethan-1-ol | HCID 2734090 | — |
| 생성물 | 1-[3-(2-Hydroxyethyl)phenyl]-2-pyrrolidinone | HCID 57444361 | 15% |
반응 단계
The title compound was prepared in 15% yield according to the general procedure for the preparation of the amides, ureas and carbamates (Method A) starting from 2-(3-bromophenyl)ethanol and 2-pyrrolidinone. Purification was achieved by flash chromatography on silica gel eluting with ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07732600B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-bbab621c1e3b4c94b45ab537ff5a5d8b |
| 출처 메모 | uspto-grants-2010_06 |