5-(3-nitrophenyl)tetrazole → HCID 178507542, 화합물

HRID 1588026노트

반응식

HRID 1588026 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:7]=[CH:8][CH:9]=1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:7]=[CH:8][CH:9]=1

참가 물질

4

반응물 1

HCID 2851295-(3-nitrophenyl)tetrazole

생성물 1

HCID 178507542HCID 178507542, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

3-Nitro-(1H-tetrazol-5-yl)benzene was dissolved in 200 ml of ethanol, treated with 1.7 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 2 hours. The reaction mixture was filtered through Celite and concentrated to give 4.7 g of the title compound.

후처리

  1. filtrationThe reaction mixture was filtered through Celite
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-8011f81aac654496807dfbdc36505afe
출처 데이터셋
uspto-grants-1993_06
특허 번호
US05220018

반응 노트

불러오는 중…