N-Acetyl-3-nitrobenzamide → HCID 19756851, 화합물
반응식
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]([NH:12][C:13](=[O:15])[CH3:14])=[O:11])[CH:7]=[CH:8][CH:9]=1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:10]([NH:12][C:13](=[O:15])[CH3:14])=[O:11])[CH:7]=[CH:8][CH:9]=1참가 물질
4
실험 절차
3-Nitro-N-(acetyl)phenylcarboxamide (200 mg) was dissolved in 60 ml of ethanol, treated with 200 mg of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 15 minutes. The reaction mixture was filtered through Celite and concentrated to give the title compound in quantitative yield as a white solid.
후처리
- filtrationThe reaction mixture was filtered through Celite
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-45d592fa32ba4835900a3cf29d733928
- 출처 데이터셋
- uspto-grants-1993_06
- 특허 번호
- US05220018
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