1-(Methylsulphonylaminocarbonyl)-3-nitrobenzene → 1-(Methylsulphonylaminocarbonyl)-3-aminobenzene
반응식
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]([NH:12][S:13]([CH3:16])(=[O:15])=[O:14])=[O:11])[CH:7]=[CH:8][CH:9]=1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:10]([NH:12][S:13]([CH3:16])(=[O:15])=[O:14])=[O:11])[CH:7]=[CH:8][CH:9]=1참가 물질
4
실험 절차
3-Nitro-N-(methanesulfonyl)phenylcarboxamide (1.6 g) was dissolved in 50 ml of ethanol, treated with 510 mg of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 15 minutes. The reaction mixture was filtered through Celite and concentrated to give the title compound (1.1 g) as a white solid.
후처리
- filtrationThe reaction mixture was filtered through Celite
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-82c4bf63241142d49f5adee5b6a3311a
- 출처 데이터셋
- uspto-grants-1993_06
- 특허 번호
- US05220018
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