Triethylamine → Cobalt octoate

HRID 1588081

반응식

HRID 1588081 반응식
[CH2:1](N(CC)CC)[CH3:2].C([CH:10]([CH2:15][CH2:16][CH2:17]C)[CH2:11][C:12]([OH:14])=[O:13])C.[N+]([O-])([O-])=O.[Co+2:23].[N+]([O-])([O-])=O>C1CCCCC1>[CH3:17][CH2:16][CH2:15][CH2:10][CH:11]([C:12]([O-:14])=[O:13])[CH2:1][CH3:2].[CH3:17][CH2:16][CH2:15][CH2:10][CH:11]([C:12]([O-:14])=[O:13])[CH2:1][CH3:2].[Co+2:23]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 25000Cobalt dinitrateHCID 1397153-Ethylheptanoic acid

생성물 1

HCID 8696Cobalt octoate수율 55.5%

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

Using a 1 liter flask, 0.40 mol triethylamine is added with stirring at room temperature to 0.40 mol 2-ethyl hexane carboxylic acid. After the exothermic reaction has abated, the reaction mixture is diluted with 65 ml cyclohexane and 0.20 mol cobalt nitrate is added. After stirring for 30 minutes, the reaction solution is filtered, leaving a 55.5% blue cobalt octoate solution in cyclohexane.

후처리

  1. customAfter the exothermic reaction
  2. additionis added
  3. filtrationthe reaction solution is filtered

출처 및 근거

ORD 기록
ord-ae8fdf9f837b4f1f9f9691ad0a891fb6
출처 데이터셋
uspto-grants-1993_06
특허 번호
US05220045

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