Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4,6-dimethoxy-1,3,5-triazine → 1-(2-Biphenylylsulfonyl) 3-(4,6-dimethoxy-1,3,5-triazin-2-yl)thiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4,6-dimethoxy-1,3,5-triazine | HCID 27840 | — |
| 반응물 | 2-Phenylbenzenesulfonyl isothiocyanate | HCID 13422027 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-(2-Biphenylylsulfonyl) 3-(4,6-dimethoxy-1,3,5-triazin-2-yl)thiourea | HCID 13422028 | 81.2% |
반응 단계
15.6 g of 2-amino-4,6-dimethoxy-1,3,5-triazine were suspended in 300 ml of dry toluene, and 27.5 g of 2-phenylbenzenesulfonyl isothiocyanate were added. The mixture was heated under reflux for 8 hours. After cooling, the resulting precipitate was collected by filtration and recrystallized from ethanol to give 35 g of 1-(2-biphenylylsulfonyl) 3-(4,6-dimethoxy-1,3,5-triazin-2-yl)thiourea represented by the following formula: ##STR28##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04568381 |
| 출처 데이터셋 | uspto-grants-1986_02 |
| ORD ID | ord-525af155c139434cbe0271954b398de2 |
| 출처 메모 | uspto-grants-1986_02 |