Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → Acrylamide-acrylic acid resin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Acrylamide | HCID 6579 | — |
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Acrylamide-acrylic acid resin | HCID 62693 | — |
반응 단계
To a stainless steel beaker was charged 214 g. of glacial acrylic acid (Rohm and Haas Production Grade). While stirring with a magnetic stirrer, 29% aqueous ammonia (technical) was added and the temperature was maintained at ≤35° C. until the pH became 7.5 (about 1.5 hours). Distilled water was added to bring the total weight to 428 g. The solution was transferred to a 1 liter glass beaker and while stirring 1.07 g. of methone was added (0.5% based on the acrylic acid). It dissolved in about 10 minutes. Then 23 g. of 50% acrylamide was added and the procedure of Examples 29-38 was followed to emulsion polymerize the monomers.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04568731 |
| 출처 데이터셋 | uspto-grants-1986_02 |
| ORD ID | ord-9f5b74bbd6364ac683a742da4d0ffb71 |
| 출처 메모 | uspto-grants-1986_02 |