Benzyl Bromide → 2-(6-Benzyloxy-2,5,7,8-tetramethylchroman-2-yl)ethanol

반응식

[OH:1][C:2]1[C:3]([CH3:18])=[C:4]2[C:9](=[C:10]([CH3:13])[C:11]=1[CH3:12])[O:8][C:7]([CH2:15][CH2:16][OH:17])([CH3:14])[CH2:6][CH2:5]2.[CH2:19](Br)[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH2:19]([O:1][C:2]1[C:3]([CH3:18])=[C:4]2[C:9](=[C:10]([CH3:13])[C:11]=1[CH3:12])[O:8][C:7]([CH2:15][CH2:16][OH:17])([CH3:14])[CH2:6][CH2:5]2)[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

참가 물질

반응물 2

HCID 7498Benzyl Bromide

HCID 118070842,5,7,8-Tetramethyl-6-hydroxy-2-(hydroxyethyl)chroman

생성물 1

HCID 109698772-(6-Benzyloxy-2,5,7,8-tetramethylchroman-2-yl)ethanol

실험 절차

Following the procedure described in Preparation 1, 2-(6-hydroxy-2,5,7,8-tetramethylchroman-2-yl)ethanol was reacted with benzyl bromide and treated and purified to give the title compound.

후처리

additiontreated
custompurified

출처 및 근거

ORD 기록: ord-ae44596f4d4741ccb6865b96fca99299
출처 데이터셋: uspto-grants-1986_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04572912

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