Methanol → Methyl 2-hydroxyhexadecanoate

HRID 1591027

반응식

HRID 1591027 반응식
[OH:1][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[C:3]([OH:5])=[O:4].[CH3:20]O>>[CH3:20][O:4][C:3](=[O:5])[CH:2]([OH:1])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

참가 물질

3

반응물 2

HCID 887MethanolHCID 928362-Hydroxyhexadecanoic acid

생성물 1

HCID 543716Methyl 2-hydroxyhexadecanoate수율 85%

실험 절차

2-hydroxyhexadecanoic acid (10.0 g, 0.0367 moles) and 8.40 g acidic resin were refluxed in 250 mls methanol for 20 hours. The solution was decolorized, filtered and concentrated giving a white solid (yield=85%)

후처리

  1. filtrationfiltered
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-931cb76f7779419398ddc2461d22b15d
출처 데이터셋
uspto-grants-1993_04
특허 번호
US05206020

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