Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester → {4-[(5-Chloro-3-methyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester | HCID 2756377 | — |
| 반응물 | 5-Chloro-3-methylpicolinaldehyde | HCID 72214055 | — |
| 생성물 | {4-[(5-Chloro-3-methyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester | HCID 58996945 | — |
반응 단계
Yellow oil prepared from (4-amino-butyl)-methyl-carbamic acid tert-butyl ester and 5-chloro-3-methyl-pyridine-2-carbaldehyde. 1H NMR (CDCl3) δ 1.44 (s, 9H), 1.50-1.60 (m, 4H), 2.27(s, 3H), 2.30-2.36 (m, 2H), 2.83 (s, 3H), 3.20-3.26 (m, 2H), 3.83 (s, 2H), 8.34 (d, 1H, J=1.5 Hz), 7.4 (d, 1H, J=1.9 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07291631B2 |
| 출처 데이터셋 | uspto-grants-2007_11 |
| ORD ID | ord-d9f7134e6b08490fb92ae823ae5d5a69 |
| 출처 메모 | uspto-grants-2007_11 |