Water → 2-Propylphenylcyanamide
반응식
[N:1]#[C:2]Br.[CH2:4]([C:7]1[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=1[NH2:9])[CH2:5][CH3:6].O>CCOCC>[CH2:4]([C:7]1[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=1[NH:9][C:2]#[N:1])[CH2:5][CH3:6]참가 물질
5
실험 절차
A mixture of cyanogen bromide (1.89 g, 17.9 mmol), and 2-n-propylaniline (3.87 g, 28.65 mmol) in ether (50 mL) was stirred for 2.5 hours under nitrogen atmosphere. The mixture was poured into water and extracted with diethylether. The solvent was dried over magnesium sulfate and concentrated in vacuo at room temperature to give 2-propylphenylcyanamide (1.2 g, 26%) as an off white solid.
후처리
- extractionextracted with diethylether
- dry with materialThe solvent was dried over magnesium sulfate
- concentrationconcentrated in vacuo at room temperature
출처 및 근거
- ORD 기록
- ord-4227c0cc5cf84acc8fa4360479d5298b
- 출처 데이터셋
- uspto-grants-2007_11
- 특허 번호
- US07297713B2
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