Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178496563, 화합물 → HCID 178496562, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178496563 | HCID 178496563 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178496562 | HCID 178496562 | 91.2% |
반응 단계
A mixture of cis-3-nitro-1-(4-methoxycyclohexylmethyl)-4-methyl-2-pyridone (0.16 g, 0.57 mmol) and 10% Pd/C (0.06 g) in ethanol was hydrogenated at 50 psi in a Parr apparatus for 22 hours. The catalyst was removed by filtration, and the solvent was evaporated to give cis-3-amino-1-(4-methoxycyclohexylmethyl)-4-methyl-2-pyridone (0.13 g, 0.52 mmol, 91%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06284768B1 |
| 출처 데이터셋 | uspto-grants-2001_09 |
| ORD ID | ord-1f9f8a207409435394372a044b20aa43 |
| 출처 메모 | uspto-grants-2001_09 |