4-Toluenesulfonyl chloride → HCID 21706748, 화합물

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[CH2:12][CH2:11][CH2:10][NH:9]2)[CH:5]=[CH:6][CH:7]=1.[C:13]1([CH3:23])[CH:18]=[CH:17][C:16]([S:19](Cl)(=[O:21])=[O:20])=[CH:15][CH:14]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[CH2:12][CH2:11][CH2:10][N:9]2[S:19]([C:16]2[CH:17]=[CH:18][C:13]([CH3:23])=[CH:14][CH:15]=2)(=[O:21])=[O:20])[CH:5]=[CH:6][CH:7]=1

참가 물질

반응물 2

HCID 73974-Toluenesulfonyl chloride

HCID 45798062-(3-chlorophenyl)pyrrolidine

생성물 1

HCID 21706748HCID 21706748, 화합물

실험 절차

The title compound, off-white solid, m.p. 107° C. and MS: m/e=335 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-(3-chloro-phenyl)-pyrrolidine and toluene-4-sulfonyl chloride.

출처 및 근거

ORD 기록: ord-96918d2208104b07887a995cfc9dbe40
출처 데이터셋: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06284785B1

반응 노트

불러오는 중…