4-Chlorobenzenesulfonyl chloride → HCID 21706776, 화합물

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[CH2:12][CH2:11][CH2:10][NH:9]2)[CH:5]=[CH:6][CH:7]=1.[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([S:20](Cl)(=[O:22])=[O:21])=[CH:16][CH:15]=1>>[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([S:20]([N:9]2[CH2:10][CH2:11][CH2:12][CH:8]2[C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=2)(=[O:22])=[O:21])=[CH:16][CH:15]=1

참가 물질

반응물 2

HCID 73984-Chlorobenzenesulfonyl chloride

HCID 45798062-(3-chlorophenyl)pyrrolidine

생성물 1

HCID 21706776HCID 21706776, 화합물

실험 절차

The title compound, light brown solid, m.p. 99° C. and MS: m/e=355 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-(3-chloro-phenyl)-pyrrolidine and 4-chloro-benzenesulfonyl chloride.

출처 및 근거

ORD 기록: ord-6a12d5b9dbbf4d828cda06d529bb356e
출처 데이터셋: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06284785B1

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