4-Toluenesulfonyl chloride → HCID 21706706, 화합물

반응식

[S:1]1[CH:5]=[CH:4][C:3]([CH:6]2[CH2:10][CH2:9][CH2:8][NH:7]2)=[CH:2]1.[C:11]1([CH3:21])[CH:16]=[CH:15][C:14]([S:17](Cl)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[S:1]1[CH:5]=[CH:4][C:3]([CH:6]2[CH2:10][CH2:9][CH2:8][N:7]2[S:17]([C:14]2[CH:15]=[CH:16][C:11]([CH3:21])=[CH:12][CH:13]=2)(=[O:19])=[O:18])=[CH:2]1

참가 물질

반응물 2

HCID 73974-Toluenesulfonyl chloride

HCID 39886722-(Thiophen-3-yl)pyrrolidine

생성물 1

HCID 21706706HCID 21706706, 화합물

실험 절차

The title compound, white solid, m.p. 114° C. and MS: m/e=308.2 (M+H+) was prepared in accordance with the general method of example 1e from (RS)-2-thien-3-yl-pyrrolidine and toluene-4-sulfonyl chloride.

출처 및 근거

ORD 기록: ord-2d47defc14c5418488acd0223acccad8
출처 데이터셋: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06284785B1

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