HCID 21706235, 화합물 → HCID 21706239, 화합물

반응식

[CH2:1]([C:4]1([C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([O:18][CH3:19])[CH:13]=2)[O:9][CH2:8][CH2:7][N:6]([CH3:10])[C:5]1=[O:11])[CH:2]=[CH2:3]>CO>[CH3:19][O:18][C:14]1[CH:13]=[C:12]([C:4]2([CH2:1][CH2:2][CH3:3])[O:9][CH2:8][CH2:7][N:6]([CH3:10])[C:5]2=[O:11])[CH:17]=[CH:16][CH:15]=1

참가 물질

실험 절차

2-Allyl-2-(-3-methoxy-phenyl)-4-methyl-morpholine-3-one, as described above in Step C, (0.400 g, 1.53 mmol) was dissolved in MeOH (20 mL), the solution purged with Ar, treated with 10% Pd/C (0.060 g), and hydrogenated under a H2 balloon. After 2 h the reaction mixture was filtered through a celite pad and concentrated to dryness to give the title compound.

후처리

customthe solution purged with Ar
additiontreated with 10% Pd/C (0.060 g)
filtrationAfter 2 h the reaction mixture was filtered through a celite pad
concentrationconcentrated to dryness

출처 및 근거

ORD 기록: ord-d1d3b5cce53d45f086f6e6e65979d9f2
출처 데이터셋: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06284755B1

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참가 물질

반응물 1

HCID 21706235HCID 21706235, 화합물

생성물 1

HCID 21706239HCID 21706239, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

후처리

customthe solution purged with Ar
additiontreated with 10% Pd/C (0.060 g)
filtrationAfter 2 h the reaction mixture was filtered through a celite pad
concentrationconcentrated to dryness

출처 및 근거

ORD 기록: ord-d1d3b5cce53d45f086f6e6e65979d9f2
출처 데이터셋: uspto-grants-2001_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06284755B1

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불러오는 중…