Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Fluoroaniline → Methyl 4-(2-fluorophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Fluoroaniline | HCID 9584 | — |
| 반응물 | Methyl 4-chloro-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate | HCID 57886211 | — |
| 생성물 | Methyl 4-(2-fluorophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate | HCID 66674390 | 61% |
반응 단계
The title compound was prepared in 61% yield by the procedure as previously described in Example 166 (step H) using methyl 4-chloro-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate (109 mg, 0.54 mmol, prepared as previously described in Example 1 (steps A-G) and 2-fluoroaniline (0.053 mL, 0.54 mmol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07732616B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-e3d3226b93d840e1a9ed91970ad037b0 |
| 출처 메모 | uspto-grants-2010_06 |