6-Chloro-2,3-dihydro-1h-indole → HCID 18932828, 화합물

HRID 1597981

반응식

HRID 1597981 반응식
[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([CH2:6][CH2:7][NH:8]2)=[CH:4][CH:3]=1.Cl[C:12]1[C:21]2[C:16](=[CH:17][C:18]([CH3:22])=[CH:19][CH:20]=2)[N:15]=[CH:14][N:13]=1>>[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([CH2:6][CH2:7][N:8]2[C:12]2[C:21]3[C:16](=[CH:17][C:18]([CH3:22])=[CH:19][CH:20]=3)[N:15]=[CH:14][N:13]=2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 2585676-Chloro-2,3-dihydro-1h-indoleHCID 219420144-Chloro-7-methylquinazoline

생성물 1

HCID 18932828HCID 18932828, 화합물수율 14%

실험 절차

Utilizing a procedure analogous to that described in Example 24, this product was prepared in 14% yield from 6-chloro-indoline and 4-chloro-7-methyl-quinazoline. (M.P. 265° C.; LC-MS: 296 (MH+)).

출처 및 근거

ORD 기록
ord-d15271c5b91a485cbc9bf11aa60987ad
출처 데이터셋
uspto-grants-1998_04
특허 번호
US05736534

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