Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-4-methoxyphenol → Methyl 3,5-dinitro-4-(2'-chloro-4'-methoxyphenoxy)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-4-methoxyphenol | HCID 87459 | — |
| 반응물 | Methyl 4-chloro-3,5-dinitrobenzoate | HCID 96161 | — |
| 반응물 | Potassium 2-chloro-4-methoxyphenolate | HCID 23716091 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Methyl 3,5-dinitro-4-(2'-chloro-4'-methoxyphenoxy)benzoate | HCID 18349326 | 66% |
반응 단계
The dinitro precursor was prepared by reacting 2-chloro-4-methoxyphenol (Aldrich Chemical Co., Milwaukee, Wis.) as the potassium 2-chloro-4-methoxyphenolate with methyl 4-chloro-3,5-dinitrobenzoate, as described in Example 1.2.1. The methyl 3,5-dinitro-4-(2'-chloro-4'-methoxyphenoxy)benzoate product (66% yield) was crystallized from ethanol to give orange crystals. Melting point: 116°-119° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05736576 |
| 출처 데이터셋 | uspto-grants-1998_04 |
| ORD ID | ord-b7823c37ff8c444d9373864ca58fd723 |
| 출처 메모 | uspto-grants-1998_04 |