Oxalyl chloride → 3-(4-Methylphenyl)propanoyl chloride

HRID 1599471노트

반응식

HRID 1599471 반응식
[C:1](Cl)(=O)[C:2]([Cl:4])=[O:3].[CH3:7][C:8]1[CH:13]=[CH:12][C:11]([CH2:14]CC(O)=O)=[CH:10][CH:9]=1>ClCCl>[CH3:7][C:8]1[CH:13]=[CH:12][C:11]([CH2:14][CH2:1][C:2]([Cl:4])=[O:3])=[CH:10][CH:9]=1

참가 물질

4

반응물 2

HCID 65578Oxalyl chlorideHCID 739273-(p-Tolyl)propionic acid

생성물 1

HCID 130292003-(4-Methylphenyl)propanoyl chloride

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

반응 조건

온도
20 °C

실험 절차

A solution of oxalyl chloride (5 ml) in dichloromethane (5 ml) was added dropwise to a solution of 3-(4-methylphenyl)propionic acid (1.5 g) in dichloromethane (20 ml). The mixture was stirred at 20° C. for 16 hours and then evaporated to give 3-(4-methylphenyl)propionyl chloride as an oil.

후처리

  1. customevaporated

출처 및 근거

ORD 기록
ord-8003302ee8fe4e75926472882c33d452
출처 데이터셋
uspto-grants-1998_04
특허 번호
US05741800

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