1,3-Bis(aminomethyl)cyclohexane → 1,3-Benzenedimethanamine
반응식
[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH2:6][CH:5]([CH2:9][NH2:10])[CH2:4]1>C1(C)C=CC=C(C)C=1>[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH2:6][CH:5]([CH3:9])[CH2:4]1.[CH3:9][C:5]1[CH:4]=[C:3]([CH:8]=[CH:7][CH:6]=1)[CH2:2][NH2:1].[C:5]1([CH2:9][NH2:10])[CH:6]=[CH:7][CH:8]=[C:3]([CH2:2][NH2:1])[CH:4]=1참가 물질
5
실험 절차
As a result of analysis by gaschromatography, it was found that the yield of 1,3-bis(aminomethyl)cyclohexane was 94.0 mol %, and as other products 0.5 mol % of metaxylene, 3.7 mol % of 3-aminomethyl-1-methylcyclohexane, 1.7 mol % of 3-methylbenzylamine and 0.1 mol % of unreacted metaxylylenediamine were obtained.
후처리
- customAs a result of analysis by gaschromatography, it
출처 및 근거
- ORD 기록
- ord-d2a65e771ade496c8d8da8007f8fbd10
- 출처 데이터셋
- uspto-grants-1998_04
- 특허 번호
- US05741928
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