Formaldehyde → Methyl 2-(N-methylenamino)-2-methylbutyrate
반응식
[NH2:1][C:2]([CH3:9])([CH2:7][CH3:8])[C:3]([O:5][CH3:6])=[O:4].[CH2:10]=O>CCOCC>[CH2:10]=[N:1][C:2]([CH3:9])([CH2:7][CH3:8])[C:3]([O:5][CH3:6])=[O:4]참가 물질
4
실험 절차
To methyl 2-amino-2-methylbutyrate (2.62 g) was dropped at room temperature 37% formalin (2.27 g), and the mixture was stirred for 4 h. Then the reaction mixture was dissolved in ether and washed with water. The organic phase was dried over magnesium sulfate, filtered and evaporated to get the captioned compound (2.80 g).
후처리
- washwashed with water
- dry with materialThe organic phase was dried over magnesium sulfate
- filtrationfiltered
- customevaporated
출처 및 근거
- ORD 기록
- ord-68a473c1f9ff4ba9bb8af051b7713fc6
- 출처 데이터셋
- uspto-grants-1999_11
- 특허 번호
- US05977025
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