Mls000756500 → 3-Amino-N-3-pyridinylbenzamide
반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8])([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8]참가 물질
4
실험 절차
A solution of 3-(3-nitrobenzoylamino)-pyridine (2 g, 8.23 mmol) in ethanol (200 ml) was treated with 10% palladium on charcoal (0.5 g) and hydrogenated at atmospheric pressure for 4 h. Filtration and evaporation afforded the product as a white solid (1.51 g, 86%)
후처리
- filtrationFiltration and evaporation
출처 및 근거
- ORD 기록
- ord-e7840f65ed22430b878c7d0c4872fc70
- 출처 데이터셋
- uspto-grants-1999_11
- 특허 번호
- US05990133
반응 노트
불러오는 중…