82-83-7 → Puberulic Acid

HRID 1603956노트

반응식

HRID 1603956 반응식
[CH:1]1[C:7](=[O:8])[C:6]([OH:9])=[C:5]([OH:10])[C:4]([OH:11])=[C:3]2C([O:14][C:15](=[O:16])[C:2]=12)=O>O>[CH:1]1[C:7](=[O:8])[C:6]([OH:9])=[C:5]([OH:10])[C:4]([OH:11])=[CH:3][C:2]=1[C:15]([OH:16])=[O:14]

참가 물질

3

반응물 1

HCID 5468472382-83-7

생성물 1

HCID 592860Puberulic Acid수율 67.9%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

5 mg of puberulonic acid are dissolved in 300 μl of water and treated at 105° for 15 hours under nitrogen, using a Pico-tag apparatus (Waters-Millipore). The reaction solution is freeze dried, obtaining about 3 mg of puberulic acid.

후처리

  1. additiontreated at 105° for 15 hours under nitrogen
  2. customdried

출처 및 근거

ORD 기록
ord-7713182a298c4b9a81c1c5d6ea67369a
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05990160

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