Serinol → 5-Amino-3-acetoxymethyl-N-(1,3-dihydroxyprop-2-yl)-2,4,6-triiodobenzamide

HRID 1604185

반응식

HRID 1604185 반응식
[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7](Cl)=[O:8].[NH2:19][CH:20]([CH2:23][OH:24])[CH2:21][OH:22]>>[NH2:1][C:2]1[C:3]([I:18])=[C:4]([CH2:13][O:14][C:15](=[O:17])[CH3:16])[C:5]([I:12])=[C:6]([C:10]=1[I:11])[C:7]([NH:19][CH:20]([CH2:23][OH:24])[CH2:21][OH:22])=[O:8]

참가 물질

3

반응물 2

HCID 68294SerinolHCID 184293385-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride

생성물 1

HCID 184293075-Amino-3-acetoxymethyl-N-(1,3-dihydroxyprop-2-yl)-2,4,6-triiodobenzamide수율 95%

실험 절차

5-Amino-3-acetoxymethyl-2,4,6-triiodobenzoyl chloride was reacted with serinol according to the conditions in Example 24g. The product was isolated in 95% yield.

후처리

  1. customThe product was isolated in 95% yield

출처 및 근거

ORD 기록
ord-ac2bf6da4a234eaabbabd1ab636b9acd
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05993780

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