Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → N,N-Diethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | N,N-Diethyl-1-naphthamide | HCID 229388 | — |
| 생성물 | N,N-Diethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide | HCID 15828028 | 71% |
반응 단계
N,N-Diethyl-1-naphthalenecarboxamide was reacted with 2 eq TMSCl according to General Method A. The resulting reaction mixture was worked up in the usual manner, then purified by chromatography with 20% ethyl acetate/80% hexanes to afford 2.1 g of the desired compound as a clear oil, a 71% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05994270 |
| 출처 데이터셋 | uspto-grants-1999_11 |
| ORD ID | ord-3e590ffdfe7c427881eabbc3eee42cca |
| 출처 메모 | uspto-grants-1999_11 |