Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → N-Ethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | N-ethyl-1-naphthalenecarboxamide | HCID 4088726 | — |
| 생성물 | N-Ethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide | HCID 19602329 | 58% |
반응 단계
N-Ethyl-1-naphthalenecarboxamide was reacted with 2 eq TMSCl according to General Method C. The resulting reaction mixture was worked up in the usual manner, then purified by recrystallization from cold ethyl acetate/hexanes to afford 1.6 g of desired compound as a white solid, a 58% yield. m.p. 141-143° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05994270 |
| 출처 데이터셋 | uspto-grants-1999_11 |
| ORD ID | ord-632443465f9a46ed8b8d291916272c7f |
| 출처 메모 | uspto-grants-1999_11 |